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Special gas chromatograph for liquefied gas dimethyl ether detection
Special gas chromatograph for liquefied gas dimethyl ether detection
Product details

Product Introduction


Product Introduction

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Liquefied petroleum gas is a basic chemical raw material and a new type of fuel, mainly composed of butene, propylene, butane, and propane. It is filled in steel cylinders and sealed with ordinary rubber materials.

Dimethyl ether is mostly produced by dehydration of formaldehyde and has similar characteristics to liquefied petroleum gas, making it suitable for use as a clean fuel. Through experiments, it has been found that dimethyl ether has swelling properties for some rubber materials, which can reduce the sealing performance of rubber materials. So the sealing material for dimethyl ether needs to be selected from special rubber materials, and the bottle body of the filling bottle should be clearly marked with the word dimethyl ether.

However, in the market, the price per ton of liquefied dimethyl ether is much lower than that of liquefied petroleum gas, so there are illegal vendors who mix dimethyl ether with liquefied petroleum gas for filling and selling, illegally profiting. If liquefied petroleum gas containing dimethyl ether is used for long-term filling, it will cause liquefied gas leakage due to the swelling effect of dimethyl ether on rubber seals, posing a threat to people's life safety. Therefore, the national standardGB 11174-2011 "Liquefied Petroleum Gas"It is prohibited to mix dimethyl ether with liquefied petroleum gas, but it is stipulated to use gas chromatography to detect the composition of liquefied petroleum gas.

The specialized gas chromatography analyzer for liquefied petroleum gas launched by Tate Instruments can quickly detect the composition and content of liquefied petroleum gas within 15 minutes, helping users quickly check whether dimethyl ether and methanol are mixed in liquefied gas, and assisting liquefied gas stations in quality control of incoming liquefied gas.


Product Characteristics

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Product Parameters

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base

stem or root of plants

join

number

Instrument model

GC2030Plus

Main purpose

Qualitative and quantitative analysis of organic compounds (inorganic gases)

Working environment requirement

Temperature requirement: 15 ℃ -35 ℃

Humidity requirement: 25% -80%

Power requirements: AC220V ± 10%, 50Hz

Power requirements

0.01℃

External dimensions

600×540×455mm

weight

About 60kg


host

machine

Temperature controlled zone

6-way independent temperature control

circuit design

Adopting ARM embedded design and internal CAN mode, the temperature control adopts a high-frequency feedback mechanism of 1700 times per second, resulting in higher control accuracy

monitor

7-inch color touch screen display, switching between Chinese and English, intelligent human-machine dialogue

injection port

Can be equipped with 3 injectors (filled injection port, split/non split capillary injection port)

detector

Multiple selection of 4 detectors (FID, TCD, FPD, ECD, NPD, PID) is possible

Auxiliary sampling device

Optional injection valve, headspace sampler, thermal analysis sampler, automatic sampler, etc

Chromatography software

Tetchrom ® The fully reverse control network chromatography workstation can automatically obtain the IP and MAC addresses of the chromatograph, and can achieve network self diagnosis. The instrument can be connected to the network to achieve remote software updates, firmware "one click updates" and other functions

Connection method

Network port connection, can also choose analog output ports such as 485, and can achieve fast communication and connection of DCS online instruments through the MUDBAS (TCP/IP) protocol

Intelligent

Equipped with automatic access to method files upon startup, self checking. When the chromatograph reaches the startup conditions, it automatically completes heating, ignition, preparation, automatic valve switching, sampling, post-processing, and uploads data results to the designated DCS, making it easy to meet project requirements for online monitoring

Method storage and method sequence

The instrument has a large capacity storage card of 8GB inside, which can store a large number of chromatographic methods; The method sequence can be freely edited to determine different projects or to implement actions such as automatic shutdown after testing, reducing the need for manual and ineffective waiting

power-off protection

The instrument adopts a power-off protection function, which automatically saves the set data at the moment of power failure, and can automatically heat up and ignite the instrument when it is powered on

automation

Supporting 8 external events, each event independently completes the required parameter settings and execution

Quick function

The instrument has quick testing functions such as one key preparation, one key cooling, one key operation, and one key ignition, greatly saving customers' ineffective waiting time

expand

Zui has an additional 4-channel input/output design, making it easy to start the chromatograph through external devices or external events. Output modes: IO passive contacts or 24V output


column

box

Temperature rise and fall

Equipped with rapid heating and cooling functions

oven temperature

5 ℃ to 450 ℃ above room temperature (up to -50 ℃ when using liquid CO2 and -99 ℃ when using liquid nitrogen)

TPD

21st level 21 platform

zuiHigh heating rate

120℃ / min

Temperature setting accuracy

0.1℃

precision

0.02℃

Temperature Stability

For every 1 ℃ change in ambient temperature, the temperature change in the column temperature chamber is less than 0.01 ℃

Cooling rate

Reduce from 350 to 50 ℃ ≤ 8 minutes (room temperature 25 ℃)

over temperature protection

When the temperature inside the column temperature box is too high, activate the automatic protection function

zuiLarge running time

9999.99 minutes


advance

appearance

system

interconnected system

Basic parameters

Number of injection ports:zuiMultiple independent temperature controlled injection units (injection port/injection valve) can be installed simultaneously

Temperature range of injection port:zuiHigh temperature of 420 ℃, with a heating setting of 1 ℃ step

Type of injection unit: single/double packed column injection port, split/non split injection port, wide aperture injection port

split/splitless

Capillary column injection port

Purpose: Used for injection into capillary chromatography columns, often used for trace impurity determination

Injection valve

High temperature tracing valve box:zuiMulti controllable 4-way multi way valve, up to 225 degrees


inspect

measure

implement

one

first

Basic parameters

Four independent temperature controlled detectors can be installed simultaneously, and the gas of the detectors is controlled by a manual pressure control system. The data acquisition rate of the detectors iszuiUp to 250Hz (4ms)

thermal conductivity detector

(TCD)

zuiHigh operating temperature: 300 ℃

Method: Dual arm microporous hot wire design

Sensitivity: S value ≥ 8000mv.ml/mg (benzene)

Baseline noise: ≤ 10UV

Baseline drift: ≤ 50UV/30min

Dynamic range: 105


colour

table

control

make

soft

piece

Tetchrom chromatography

workstation

Suitable for operating systems such as Win7 and Win10, it reads sampling data from CDF files that comply with A/A (American Society for Analysis) standards

data acquisition

A self-developed anti control network chromatography workstation that enables simultaneous acquisition and control of three channel data (software copyright certificate provided)

Rights Management

Can achieve three-level permission management for operation and maintenance personnel, instrument users, and equipment administrators

data transmission

By using Ethernet communication, the data throughput is faster and the bidirectional handshake frequency is higher. The chromatography system with completely independent intellectual property rights has a standard interface of MODBUS/TCP, which can be easily integrated with DCS

sensitivity

1uV*s, Dynamic range: 220

Network Communications

Support wireless network communication connection

Unmanned function

Support various functions required for automated online monitoring, such as automatic startup, automatic temperature rise, automatic ignition, automatic bridge current opening, automatic sample collection, automatic data processing, and automatic generation of data trend charts

automatic calibration

For customized projects, automatic zeroing, calibration, calibration and other functions can be achieved, as well as scheduled calibration

system safety

Fully supports FDA-21CFR Part 11 authentication (electronic signature, resume, user password), System Applicability Testing (SST), and System Authentication Tools (IQ/OQ)

Batch processing function

The batch processing function enables the control of the instrument, automatic sampler sequence acquisition, automatic integration correction, and output report to be completed in one go, simplifying daily tedious analysis

data comparison

Powerful post-processing functions, including spectrum comparison, recalibration, and data input and output, are all available. "Special Attention Online" can obtain analysis results online without waiting for the end of data collection


Software Interface

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PC based network version chromatography workstation software for instrument operation(zuiSupports up to 253 units, enabling program control of instrument injection ports, column temperature chambers, and detector temperature rise and fall. Under the condition that the customer is equipped with an automatic injection valve (or automatic sampler), it is possible to achieve a series of testing processes such as unmanned instrument operation, automatic heating and ignition of the instrument, automatic loading method, and automatic calculation of test results

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Chromatogram peak chart

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