Gas chromatograph for Baijiu-Fornitore globale

Room 602, Building F, Minggu Science and Technology Park, No. 7001 Zhongchun Road, Minhang District, Shanghai

Product Introduction

Product Introduction

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The main components of Baijiu are ethanol and water, as well as acids, esters, alcohols, aldehydes and other kinds of trace organic compounds (about 1%~2% of the total). Due to different fermentation processes, the types and contents of these trace organic compounds are different, which also determine the flavor and taste style of Baijiu (such as soy sauce flavor, luzhou flavor, light flavor, rice flavor, and mixed flavor).

The components, contents and detection methods of Baijiu are specified in the National Food Safety Standard for Distilled Liquor and its Blended Liquor (GB 2757-2012), GB/T5009.48-2003, Methods of Analysis of Hygienic Standards for Distilled Liquor and Blended Liquor, and GB/T 10345-2007, Methods of Analysis for Baijiu. The detection of components of Baijiu by gas chromatography is an essential production link for liquor manufacturers.

Taite Instrument has launched a special gas chromatograph for Baijiu manufacturers, which is equipped with a special chromatographic column for Baijiu. With FID hydrogen flame particle detector, it can directly analyze the content of methanol and fusel oil in Baijiu, and can also determine the components and content of higher alcohols in Baijiu, such as n-propanol, isobutanol, n-butanol, isoamyl alcohol, n-amyl alcohol, etc. The method is simple and rapid, with good precision, and the relative deviation is less than 5%.

This equipment can help Baijiu manufacturers to control the product process, ensure the stability of Baijiu taste and quality, provide practical scientific basis for Baijiu flavor and taste, and help health and epidemic prevention stations at all levels and product quality inspection institutes to strengthen management of Baijiu market and crack down on counterfeit and inferior Baijiu products.

Product Characteristics

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Product Parameters

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base stem or root of plants join number	Instrument model	GC2030Plus
	Main purpose	Qualitative and quantitative analysis of organic compounds (inorganic gases)
	Working environment requirement	Temperature requirement: 15 ℃ -35 ℃
		Humidity requirement: 25% -80%
		Power requirements: AC220V ± 10%, 50Hz
	Power requirements	0.01℃
	External dimensions	600×540×455mm
	weight	About 60kg

host machine	Temperature controlled zone	6-way independent temperature control
	circuit design	Adopting ARM embedded design and internal CAN mode, the temperature control adopts a high-frequency feedback mechanism of 1700 times per second, resulting in higher control accuracy
	monitor	7-inch color touch screen display, switching between Chinese and English, intelligent human-machine dialogue
	injection port	Can be equipped with 3 injectors (filled injection port, split/non split capillary injection port)
	detector	Multiple selection of 4 detectors (FID, TCD, FPD, ECD, NPD, PID) is possible
	Auxiliary sampling device	Optional injection valve, headspace sampler, thermal analysis sampler, automatic sampler, etc
	Chromatography software	Tetchrom ® The fully reverse control network chromatography workstation can automatically obtain the IP and MAC addresses of the chromatograph, and can achieve network self diagnosis. The instrument can be connected to the network to achieve remote software updates, firmware "one click updates" and other functions
	Connection method	Network port connection, can also choose analog output ports such as 485, and can achieve fast communication and connection of DCS online instruments through the MUDBAS (TCP/IP) protocol
	Intelligent	Equipped with automatic access to method files upon startup, self checking. When the chromatograph reaches the startup conditions, it automatically completes heating, ignition, preparation, automatic valve switching, sampling, post-processing, and uploads data results to the designated DCS, making it easy to meet project requirements for online monitoring
	Method storage and method sequence	The instrument has a large capacity storage card of 8GB inside, which can store a large number of chromatographic methods; The method sequence can be freely edited to determine different projects or to implement actions such as automatic shutdown after testing, reducing the need for manual and ineffective waiting
	power-off protection	The instrument adopts a power-off protection function, which automatically saves the set data at the moment of power failure, and can automatically heat up and ignite the instrument when it is powered on
	automation	Supporting 8 external events, each event independently completes the required parameter settings and execution
	Quick function	The instrument has quick testing functions such as one key preparation, one key cooling, one key operation, and one key ignition, greatly saving customers' ineffective waiting time
	expand	zuiWith an additional 4-channel input/output design, it is easy to start the chromatograph or external events through external devices. Output modes: IO passive contacts or 24V output

column box	Temperature rise and fall	Equipped with rapid heating and cooling functions
	oven temperature	5 ℃ to 450 ℃ above room temperature (up to -50 ℃ when using liquid CO2 and -99 ℃ when using liquid nitrogen)
	TPD	21st level 21 platform
	zuiHigh heating rate	120℃ / min
	Temperature setting accuracy	0.1℃
	precision	0.02℃
	Temperature Stability	For every 1 ℃ change in ambient temperature, the temperature change in the column temperature chamber is less than 0.01 ℃
	Cooling rate	Reduce from 350 to 50 ℃ ≤ 8 minutes (room temperature 25 ℃)
	over temperature protection	When the temperature inside the column temperature box is too high, activate the automatic protection function
	zuiLarge running time	9999.99 minutes

advance

appearance

system

interconnected system

Basic parameters

Number of injection ports:zuiMultiple independent temperature controlled injection units (injection port/injection valve) can be installed simultaneously

Temperature range of injection port:zuiHigh temperature of 420 ℃, with a heating setting of 1 ℃ step

Type of injection unit: single/double packed column injection port, split/non split injection port, wide aperture injection port

split/splitless

Capillary column injection port

Purpose: Used for injection into capillary chromatography columns, often used for trace impurity determination

inspect

measure

implement

one

first

Basic parameters

Four independent temperature controlled detectors can be installed simultaneously, and the gas of the detectors is controlled by a manual pressure control system. The data acquisition rate of the detectors iszuiUp to 250Hz (4ms)

Hydrogen flame ionization

detector

（FID）

zuiHigh operating temperature: 420 ℃

Method: Dual channel method

Automatic ignition function: using military grade igniters, the ignition wire adopts a non exposed design, and the service life is 100 times that of conventional ignition wires, with a 10-year warranty

Detection limit: 5.0 × 10^-12G/s (n-hexadecane)

Baseline noise: ≤ 2 × 10^-14A

Baseline drift: ≤ 1 × 10^-13A/30 min (after the instrument stabilizes for 2 hours)

Dynamic range: 10⁷

colour table control make soft piece	Tetchrom chromatography workstation	Suitable for operating systems such as Win7 and Win10, it reads sampling data from CDF files that comply with A/A (American Society for Analysis) standards
	data acquisition	A self-developed anti control network chromatography workstation that enables simultaneous acquisition and control of three channel data (software copyright certificate provided)
	Rights Management	Can achieve three-level permission management for operation and maintenance personnel, instrument users, and equipment administrators
	data transmission	By using Ethernet communication, the data throughput is faster and the bidirectional handshake frequency is higher. The chromatography system with completely independent intellectual property rights has a standard interface of MODBUS/TCP, which can be easily integrated with DCS
	sensitivity	1uV*s， Dynamic range: 220
	Network Communications	Support wireless network communication connection
	Unmanned function	Support various functions required for automated online monitoring, such as automatic startup, automatic temperature rise, automatic ignition, automatic bridge current opening, automatic sample collection, automatic data processing, and automatic generation of data trend charts
	automatic calibration	For customized projects, automatic zeroing, calibration, calibration and other functions can be achieved, as well as scheduled calibration
	system safety	Fully supports FDA-21CFR Part 11 authentication (electronic signature, resume, user password), System Applicability Testing (SST), and System Authentication Tools (IQ/OQ)
	Batch processing function	The batch processing function enables the control of the instrument, automatic sampler sequence acquisition, automatic integration correction, and output report to be completed in one go, simplifying daily tedious analysis
	data comparison	Powerful post-processing functions, including spectrum comparison, recalibration, and data input and output, are all available. "Special Attention Online" can obtain analysis results online without waiting for the end of data collection

Software Interface

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The PC network version chromatography workstation software is used to operate the instrument (with a maximum support of 253 units), achieving program control of the instrument's injection port, column temperature box, and detector temperature rise and fall. Under the condition that the customer is equipped with an automatic injection valve (or automatic sampler), it is possible to achieve a series of testing processes such as unmanned instrument operation, automatic heating and ignition of the instrument, automatic loading method, and automatic calculation of test results

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Chromatogram peak chart

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