Software method:
1.1 ★Integrated control of mass spectrometer and gas chromatograph in Chinese;The synchronous scanning function can obtain both scan and sim data in one injection test, improving analysis efficiency; The alternating scanning function can be performed alternately with scan and sim, expanding the analysis function.
1.2 ★ During operation, a time interval can be set to turn off the filament and electron multiplier to protect themCan avoid solvents or other easily saturated substances that peak at intermediate moments.
1.3 The software can automatically select the characteristic ions of the target compound and group them based on the data obtained from the full scan, and save them to the analysis method without manual input;
1.4 Manual/automatic tuning, data acquisition, quantitative analysis and spectral library retrieval functions, analysis result report output;
1.5 Automatic shutdown;
1.6 Chromatographic flow monitoring; Chromatography gas cut-off, mass spectrometry ion source and transmission line automatic cooling protection, mass spectrometry stops running;
1.7 Real time monitoring of molecular pump speed and current, with abnormal prompts.
1.8 ★ Choose unlimited number of groups for ion mode detection (SIM), with a maximum of 128 ions per group.
runtime environment
1 Environmental temperature: 18-35 ℃, temperature fluctuation within 2 degrees;
2 Relative humidity: ≤ 80%;
3 Applicable power supply: 220V (± 10%), 50Hz (± 2%);
Technical parameters and indicators
1Mass spectrometry section
1.1ion source
★sensitivityEI sensitivity: 1 pg OFN S/N 600:1;
Ion source material: inert ceramic ion source, equipped with dual filaments; The maximum filament current is 400uA;
Ionization energy: 10-100eV;
Interface temperature:5Adjustable from 0 ℃ to 350 ℃, with precision better than0.1℃,The mass spectrometer is temperature controlled and does not occupy the auxiliary heating area of the gas chromatograph;
Ion source temperature: 50 ℃ -350 ℃;
1.2quality analyzer
Quality analyzer:High precision metal quadrupole with pre-set rod;
Quadrupole rod temperature: Quality stability can be ensured without temperature control;
★Quality range: 1.5-1050amu, The software can fully set and detect;
Quality axis stability: better than 0.10 amu/48 hours;
★Scanning methods: full scan, selective ion monitoring, full scan and selective ion synchronous monitoring, alternating scan;
1.3detector
Detector: Long life 13 level non continuous dynode electron multiplier;
maximumscanning speed: 10,000 amu/ s,Speed adjustable throughout the entire process;
Dynamic range: 106;
Peak area reproducibility; Automatic injection RSD ≤ 2%;
★vacuum system:mechanical pumpExtraction speed 4m ³/h; configurationHigh performance turbo molecular pump pumping speed250 L/s;
The maximum allowable flow rate of the chromatographic column is 5ml/min helium gas.
Maintainable components: detachable ion source, filament, lens, pre quadrupole, and detector;
2.2 Gas chromatograph parameters;
2.2.1column box
Temperature range: 5 degrees above room temperature˚C~450˚C;
Temperature stability; When the ambient temperature changes by 1˚At C, it is better than 0.01˚C;
★Program heating up:20step21Platform;
Heating rate: maximum heating rate 120˚C/min;
Rapid cooling time: from 300˚C--50˚C is less than 5 minutes;
2.2.2 Split/non split capillary column injection port;
最高使用温度400˚C;
Pressure setting range: 0~100 psi, control accuracy 0.01 psi;
★The injection port has pulse pressure;
2.2.3★Flow control: Electronic pneumatic control with constant current, constant pressure, program flow rate, program boost and other modes;
2.2.4 Except for the column box, the area that can be heated and temperature controlled should not be less than6It can reach a maximum temperature of 400 degrees Celsius˚C;
2.2.5 Can be configured with 16 bit, 24 bit, and 156 bit liquid automatic samplers.
2.2.6 Retention time reproducibility<0.02%.
