Beijing Dingchuang Sapphire Window Reactor Magnetic Stirring Reactor
Instrument Introduction:
Beijing Dingchuang Sapphire Window Reactor Magnetic Stirring ReactorThe sapphire window reactor and quartz window reactor are suitable for reactions that require visual observation under high pressure and reactions that require photocatalytic catalysis. This is a non-standard product that needs to be customized according to customer requirements. It can be equipped with pressure gauges, intake valves, exhaust valves, probe tubes, thermocouples, and process injection ports.
characteristic:
1. New fastening structure:
In the past, during the preparation period for each experiment of the flange fastening structure window reaction kettle sapphire reaction kettle, all bolts of the reaction kettle had to be unscrewed, and after adding the reaction materials, they had to be re tightened one by one again. The opening and sealing process of a single screw requires more than ten turns of rotation, and each reactor has multiple bolts, which is time-consuming and laborious during the testing process.
Our company's window reaction kettle sapphire reaction kettle high-pressure reaction kettle adopts a half moon ring type quick opening fastening structure. Compared with traditional institutions, when opening the reactor for each experiment, simply loosen the screw by about 1 turn to easily remove the holding ring from the side and quickly open the reactor.
The tightening process is also simple and effortless. And each holding ring bolt exerts pressure on the lower cushion ring, which then compresses the kettle head, so that the force of the bolts can be evenly distributed to the kettle head. However, traditional flange structures have strict requirements for tightening force and diagonal tightening sequence to ensure uniform force distribution, and require high operational skills from operators. A slight negligence can lead to leakage of the reaction vessel and re tightening of the seal.
2Small space double line sealed structure:
Polytetrafluoroethylene (PTFE) is widely used as an excellent corrosion-resistant material in instrument sealing processes, but it itself undergoes cold flow deformation at 250 degrees.
To overcome this contradiction, our company adopts precision machining small space double line sealing technology to control the sealing gap between the kettle head and body within a very small range. PTFE deforms at high temperatures, but the joint gap is too small for PTFE to deform and flow cold to the outside of the sealing groove. It can only deform and expand inside the groove, thereby further enhancing the sealing performance of the reaction kettle. In addition, V-shaped sealing grooves are machined on the sealing surfaces of the kettle head and body to increase the sealing area. At the specified operating temperature, the higher the temperature, the better the sealing performance of the sealing surface.
3No dead space probe:
The sample size for laboratory level reactions is generally small, and some samples are expensive. So the experimental equipment (window reactor, sapphire reactor) has a significant impact on the accuracy of experimental results and funding. For example, the wall hanging situation when adding liquid materials is a prominent issue. Our company's DC series non stirred reaction kettle uses a bottom probe tube to directly enter the kettle, without any dead space caused by an adapter in the middle. If the air inlet is changed to a ball valve, the material can be injected directly into the kettle through a syringe during the reaction. Suitable for adding trace reactants.
4Strict selection of materials:
The durability and reliability of materials are crucial for the synthesis kettle. Our company adheres to the concept of reliability and durability, and the main body of all window reaction kettles and sapphire reaction kettles is made of high-quality stainless steel materials. The standard valves and fittings are all imported brands to increase reliability.
5:
The sapphire reaction kettle in the window reactor can be equipped with a pressure relief valve, which can be set to a high operating pressure by oneself. Ensure the reliability of the reactor's use.
6Flexible selection and customization(Please refer to the relevant color page for details) All window reaction kettles and sapphire reaction kettles can accept personalized customization from customers. Window high-pressure reactor, sapphire high-pressure reactor, quartz window high-pressure reactor, also known as laboratory reactor, micro reactor, and small reactor.